Date Published: February 01, 2012
Publisher: International Union of Crystallography
Author(s): Elizaveta A. Trush, Oleg V. Shishkin, Victor A. Trush, Irina S. Konovalova, Tetyana Yu. Sliva.
The title compound, C4H12N+·C8H11NO5PS−, was obtained from tetramethylammonium hydroxide and dimethyl(phenylsulfonyl)amidophosphate. The tetramethylammonium cation has a slightly distorted tetrahedral configuration and the N—C bond lengths lie in the range 1.457 (3)–1.492 (3) Å. In the crystal, no classical hydrogen bonds are observed between the cation and the anion.
For the synthesis of sulfonylamide derivatives, see: Kirsanov & Shevchenko (1956 ▶); Pietraszkiewicz et al. (2002 ▶); Trush et al. (2009 ▶); Moroz et al. (2009 ▶); Shatrava et al. (2010 ▶). For the crystal structures of tetramethylammonium compounds, see: Cao et al. (2008 ▶); Liu et al. (2004 ▶).